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WU Jian-guo, WANG Hong-yu, WU Yan-bin, CHEN Ti-qiang. GC-MS Analysis of the Essential Oil from Ultrafine-Powder of Ganoderma sinense by Supercritical CO2 Fluid Extraction[J]. Fujian Journal of Agricultural Sciences, 2012, 27(8): 909-912.
Citation: WU Jian-guo, WANG Hong-yu, WU Yan-bin, CHEN Ti-qiang. GC-MS Analysis of the Essential Oil from Ultrafine-Powder of Ganoderma sinense by Supercritical CO2 Fluid Extraction[J]. Fujian Journal of Agricultural Sciences, 2012, 27(8): 909-912.

GC-MS Analysis of the Essential Oil from Ultrafine-Powder of Ganoderma sinense by Supercritical CO2 Fluid Extraction

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  • Received Date: February 16, 2012
  • Revised Date: March 19, 2012
  • Objective:Further to analysis chemical components in the essential oil(EO) of Ganoderma sinense. Methods:EO was extracted using Supercritical CO2 fluid extraction(SFE-CO2) technique from the ultrafine-powder of Ganoderma sinense, and detected by Gas chromatography-mass spectrometry (GC-MS). Results: 46 compounds were checked out from the EO extract(with 1.47% of extract rate, w/w), and 26 compounds(matching degree >83%) were identified representing 79. 2% of the total EO, including n-Hexadecanoic acid, (E)-9-Octadecenoic acid methyl ester, (E)-9- Octadecenoic acid and (E,E)-2,4- Decadienal, 9-Methyl-Z-10-tetradecen-1-ol acetate, 1,8,8-trimethyl-2-(3-oxocyclo- pentenyl)-Tricyclo[3.2.1.0(2,4)]octane-3,3-dicarbonitrile, (Z)-9-Octadecenoic acid-2-hydroxy-1- (hydroxymethyl) ethyl ester and E-11-Hexadecen-1-ol and so on. Collusion: The results indicated that chemical components and their relative contents of the EO extracted by SFE-CO2 were different from that by steam distillation(SD) after ether refluxing.
  • 张裕强,郭立玮,刘史佳,等. 不同方法提取荜茇挥发油的GC-MS分析[J]. 质谱学报,2008,29(4):231-236.
    陈体强,吴锦忠. 超微粉碎后超临界CO2 萃取灵芝孢子挥发油组分的GC-MS分析[J]. 天然产物研究与开发,2006a,18(6):982-985.
    CHEN T Q, ZHAO X Y, WU J Z, et al. Supercritical fluid CO2 extraction, simultaneous determination of components in ultrafine-Powder of Ganoderma sinense by HPLC-ESI-MS method[J]. Journal of the Taiwan Institute of Chemical Engineers, 2011, 42(3): 428-434.
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