Aromatics Determination of Xinbai 8 Loquat by HS-SPME Internal Standard Method

ZHANG Gui-bin; AN Ning; ZHU Li-hui; JIANG Ji-mou; HU Wen-shun

doi:10.19303/j.issn.1008-0384.2019.06.006

Volume 34 Issue 6

Sep. 2019

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ZHANG Gui-bin, AN Ning, ZHU Li-hui, JIANG Ji-mou, HU Wen-shun. Aromatics Determination of Xinbai 8 Loquat by HS-SPME Internal Standard Method[J]. Fujian Journal of Agricultural Sciences, 2019, 34(6): 660-667. doi: 10.19303/j.issn.1008-0384.2019.06.006

Citation:

ZHANG Gui-bin, AN Ning, ZHU Li-hui, JIANG Ji-mou, HU Wen-shun. Aromatics Determination of Xinbai 8 Loquat by HS-SPME Internal Standard Method[J]. Fujian Journal of Agricultural Sciences, 2019, 34(6): 660-667. doi: 10.19303/j.issn.1008-0384.2019.06.006

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Aromatics Determination of Xinbai 8 Loquat by HS-SPME Internal Standard Method

doi: 10.19303/j.issn.1008-0384.2019.06.006

ZHANG Gui-bin¹,
AN Ning¹,
ZHU Li-hui¹,
JIANG Ji-mou^{2
,
,},
HU Wen-shun^{1, 2
,
,}

1.
Horticultural College, Fujian Agricultural and Forestry University, Fuzhou, Fujian 350002, China
2.
Institute of Fruit Trees, Fujian Academy of Agricultural Sciences, Fuzhou, Fujian 350002, China

Received Date: 2019-02-12
Rev Recd Date: 2019-05-14
Publish Date: 2019-06-28

Abstract

Abstract

Objective To determine the aromatic composition of loquat fruit and cyclohexanone concentration for the HS-SPME-GC/MS internal standard method. Methods The pulp of Xinbai 8 fruits was added with a cyclohexanone solution in the concentration of 947, 94.7, 9.47, 0.947 μg·μL^-1 at a same volume as the internal standard for HS-SPME-GC/MS analysis. Results The analysis detected 10 classifications of chemicals including aldehydes, alkanes, dutrex, ketones and alcohols. Hexanal, (E)-2-hexenal, n-butyl cyclohexane, 2-heptanone, n-pentyl cyclohexane, (E)-2-hexene-1-alcohol, and styrene were the dominating volatiles among the 43 compounds identified.In the cyclohexanone-added samples, the decreasing concentration produced 31, 40, 42 and 33 aromatic substances with the effective peak area ratios of 38.20%, 28.49%, 42.70% and 39.52%, and the peak area ratios of 38.20%, 58.55%, 36.37% and 25.86%, respectively. A maximum number of aromatics was found in the sample that was added with 9.47 μg·μL^-1 cyclohexanone which also had the highest effective peak area ratio and optimum peak area radio. Conclusion The aromatics in the fruits of Xinbai 8 were diverse, and the cyclohexanone concentration at 9.47 μg·μL^-1 was the choice internal standard for the analytical.
- loquat,
- aromatics,
- cyclohexanone,
- internal standard,
- SPME,
- GC-MS

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References(24)

References

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